Nanometer-resolved quantification of mechanical response in nanoparticle-based composites
M Hennes, AM Jakob, F Lehnert, U Ross, A Lotnyk, SG Mayr
NANOSCALE | ROYAL SOC CHEMISTRY | Published : 2016
Nanocomposites constitute an upcoming class of materials that has enormous potential within a broad range of areas, particularly with regard to mechanical applications. However, the tuning of material properties requires a full understanding of the mechanical response of the nanocomposite across all length scales. While characterization from the micro to macroscale is well established at this point, quantification of mechanical behavior at the nanoscale is still an unresolved challenge. With this background, the current work demonstrates the capabilities of quantitative contact resonance atomic force microscopy (CR-AFM) to localize and reliably characterize Ni nanoparticles that are embedded..View full abstract
Awarded by Translational Center for Regenerative Medicine
The authors thank R. Fechner, Dr F. Frost, Dr M. Ehrhardt and Dr P. Lorenz for assistance during optimization of sample synthesis, M. Sarmanova for kind help with the CR-AFM setup, J. Lorbeer for providing ion-beam smoothened FS reference samples, A. Mill for TEM-lamella preparation as well as E. Wisotzki for proofreading the manuscript. We also owe thanks to Prof. Dr Dr h.c. B. Rauschenbach for general support. Research was performed within the Leipzig Graduate School of Natural Sciences "Building with Molecules and Nano-objects" (BuildMoNa), which was established within the German Excellence Initiative by the German DFG. Partial funding by the Deutsche Forschungsgemeinschaft (DFG) via the SPP 1681, as well as the Translational Center for Regenerative Medicine (BMBF 1315883) is gratefully acknowledged.