Journal article

Size and Composition Control of Magnetic Nanoparticles

Dingchen Wen, Trent Ralph, Jiho Han, Siobhan Bradley, Marcus J Giansiracusa, Valerie Mitchell, Colette Boskovic, Nicholas Kirkwood

The Journal of Physical Chemistry C: Energy Conversion and Storage, Optical and Electronic Devices, Interfaces, Nanomaterials, and Hard Matter | American Chemical Society | Published : 2023

Abstract

Magnetite nanoparticles are a type of magnetic nanoparticle (MNP) that are inexpensive to make and can be formed in different shapes and sizes. MNPs can be used in DNA/RNA purification, drug delivery, and other biomedical applications. The commonly employed solvothermal route to make these MNPs gives the most uniform products with the smallest size distribution, but there is a need to identify easily controlled changes to reaction parameters that can reliably tune the size and composition of the MNPs made by this method. In this work we report simple and reliable methods whereby adjusting the total water content and basic salt concentration affords size and composition control, respectively...

View full abstract

Grants

Awarded by ARC


Awarded by Australian Government Research Training Program (RTP) Scholarship


Awarded by Australian Research Council


Funding Acknowledgements

The authors acknowledge the ARC for support through grant CE170100026. The authors thank Prof. Paul Mulvaney and the Nanoscience Laboratory at the University of Melbourne for the use of laboratory. D.W. thanks the Australian Government for providing an Australian Government Research Training Program (RTP) Scholarship. The authors thank the Ian Holmes Imaging Centre at the Bio21 Institute for electron microscope access. Part of this work was carried out on the X-ray Absorption Spectroscopy beamline at the Australian Synchrotron, part of ANSTO (grant number M16952) . Part of this work was performed in part at the Trace Analysis for Chemical, Earth and Environmental Sciences (TrACEES) Platform at the University of Melbourne. We acknowledge the Australian Research Council for an equipment grant (LE210100009) .