Journal article

Diffraction thermometry and differential thermal analysis

EH Kisi, DP Riley

JOURNAL OF APPLIED CRYSTALLOGRAPHY | INT UNION CRYSTALLOGRAPHY | Published : 2002

Abstract

A unit-cell parameter anomaly observed during the precipitation and growth of Ti3SiC2 from a Si-substituted TiC phase is interpreted as the release of latent heat. The observations are used to propose a powder diffraction method for conducting differential thermal analysis as part of in situ phase transition studies. © 2002 International Union of Crystallography.

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